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What is the signal splitting pattern , the integrated value and chemical shift of the NMR spectrum below . The unknown is C8H8O2
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- How could 13C NMR spectroscopy be used to distinguish among isomers X, Y, and Z?57. 200 10 __100_ 140 120 6 100 S 1 13C NMR C12H12 135.39 133.91 129.97 127.39 127.20 126.21 21.69Mass Spectrum 1000 - 800.0 600.0 400.0 200.0 0.000- 50.00 100.0 m/z 150.0 200.0 lamalan saldassallaalan C-H;BRO, D00 3000 2000 1000 500 HAVENUNBERIl Abundance
- In a 300 MHz NMR spectrometer, A) what is the Larmor frequency in MHz of a 15N nucleus? g H = N 26.752; g = 2.7126; B) Using the same NMR instrument, suppose that a 13C nucleus from a sample generates a signal which has a frequency of 11,250 Hz higher than that from the carbons in TMS. What is the chemical shift of that carbon atom from the sample? A) 30 MHz; B) 0.15 ppm OA) 25 MHz; B) 0.35 ppm A) 35 MHz; B) 0.30 ppm OA) 25 MHz; B) 0.55 ppm7) The correct structure that corresponds to the spectroscopic data given below is [IR 2720, 1710 1 point cm*1. 1H NMR 9.80(s, 1H), 7.50(dd, J = 8,0Hz, 2Hz, 1H), 7.40(d, J = 2.0Hz, 1H), 6.90(d, J = 8.0Hz, 1H), 3.90(s, 3H), 3.80(s, 3H)] COOH OMe Me CHO OMe OMe CHO OMe OMe COOH OMe MeMyriam 1718 1. 4000 3000 1600 1200 800 V (cm¹) 100 Mass Spectrum 43 119 80 60 JIK M+* 40 176 20 161 C12 H16 O 40 80 200 280 120 160 m/e 13C NMR Spectrum (50.0 MHz, CDCI, solution) expansion 188 IR Spectrum (liquid film) % of base peak DEPT CH₂ CH₂ CH proton decoupled L 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) J 1 9 10 I 8 2000 160 the 1 7 6 240 120 130 130 125 ppm 125 ppm L 5 expansion 1 80 1 4 solvent Problem 99 UV Spectrum max 262 nm (log₁0 € 2.5) solvent methanol 40 t I 3 1 2 4 08 (ppm) TMS 1 0 8 (ppm) 1 1 205
- What Is the correct order (from lowest to highest ppm-value) for the chemical shifts of the labeled carbon atoms In the PC-NMR spectrum of this compound? III O 1.I <|how is H-NMR highly applicable to polymers and organic molecules.7.) From the following sets of data, please propose a reasonable structure for the unknown organic compound. This molecule is entirely composed of C, H, and N only. Please show all of your work and feel free to write on the spectra any clues as to the structure. 4000 3000 2000 1000 S DO Infrared spectrum of unknown. KBr salt plate sample. 100 MS-NU-6396 80 60 40 20 - 10 20 30 40 50 60 70 80 90 100 110 m/z Mass spectrum of unknown. Molecular ion = 83.1 Relative Intensity3c A doublet signal appeared in the 1H NMR spectrum that was analysed on 400 MHz NMR given below. Calculate the coupling constant (J) of this signal.Resolves into 13C NMR Spectrum (50.0 MHz, CDCI, solution) two signals at higher field DEPT CgH11Br Resolves into two signals at higher field expansions proton decoupled solvent 35.0 34.0 ppm 200 160 120 80 40 O 8 (ppm) 1H NMR Spectrum (200 MHz, CDCI, solution) expansion 3.0 2.5 ppm TMS 10 9 8 7 6 5 4 3 2 1 8 (ppm) Determine the structure of the compound based on the above informationWhat would be the ratio N(-1/2)/N(+1/2) of the number of protons in spin state (-1/2) over (+1/2) state at a very low temperature of 3K (liquid He boiling pt) and in a 800 MHz NMR spectrometer?SEE MORE QUESTIONS