An orange compound, dissolved in dichloromethane, is added to a chromatogra- phy column. The elution is begun using hexane as the solvent. After 6 L of solvent was passed through the column, the orange band had still not traveled down the column appreciably. What should be done to make this experiment work better.

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter29: Mass Spectrometry
Section: Chapter Questions
Problem 29.2QAP
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An orange compound, dissolved in dichloromethane, is added to a chromatogra-
phy column. The elution is begun using hexane as the solvent. After 6 L of solvent
was passed through the column, the orange band had still not traveled down the
column appreciably. What should be done to make this experiment work better.
Transcribed Image Text:An orange compound, dissolved in dichloromethane, is added to a chromatogra- phy column. The elution is begun using hexane as the solvent. After 6 L of solvent was passed through the column, the orange band had still not traveled down the column appreciably. What should be done to make this experiment work better.
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