3458 Problem 9 115 IR Spectrum (CO solution 4000 100 282 2 20 80 % of base peak W 3000 2000 V (cm) 59 103 1600 40 1200 600 1400 Move branch M-118 (<1%) Mass Spectrum Ho Gh C6H1402 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 0 MHz CDCI, solution) <- 4 =1400 2n+1=3 No significant UV absorption above 220 nm 2x61214-2)+(x2) =(12+2-12+2/14 = 12+2= 12 +4 114-14 =2016 DEPT CH CH CH proton decoupled solvent L T 200 160 120 80 40 'H NMR Spectrum (200 MHz, CDCI, solution) Exchanges with D₂O ୮ L 1451427 =148 0 8 (ppm) TMS 2 L 10 9 8 7 6 5 4 3 2 1 0 8 (pp
3458 Problem 9 115 IR Spectrum (CO solution 4000 100 282 2 20 80 % of base peak W 3000 2000 V (cm) 59 103 1600 40 1200 600 1400 Move branch M-118 (<1%) Mass Spectrum Ho Gh C6H1402 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 0 MHz CDCI, solution) <- 4 =1400 2n+1=3 No significant UV absorption above 220 nm 2x61214-2)+(x2) =(12+2-12+2/14 = 12+2= 12 +4 114-14 =2016 DEPT CH CH CH proton decoupled solvent L T 200 160 120 80 40 'H NMR Spectrum (200 MHz, CDCI, solution) Exchanges with D₂O ୮ L 1451427 =148 0 8 (ppm) TMS 2 L 10 9 8 7 6 5 4 3 2 1 0 8 (pp
Chapter13: Structure Determination: Nuclear Magnetic Resonance Spectroscopy
Section13.SE: Something Extra
Problem 29AP
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